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Vol.2 , No. 4, Publication Date: Aug. 27, 2016, Page: 25-34
 along with Citric acid and Sodium hypophosphite as catalyst applied on cotton fabric by pad-dry-cure method. Spectrophotometer analysis of combined dyed and finished cotton fabric show a deeper color yield and good aroma finishing using monochlorotriazine reactive dye along with jasmine oil microencapsulated in beta cyclodextr in in presence of citric acid and sodium hypophosphite applied on cotton fabric. For comparison purpose, beta cyclodextrin encapsulated aroma finish was also applied after dyeing cotton fabric with the same monochlorotriazine on cotton fabric in conventional two stage process. Simultaneous reactive dyeing and aroma finishing with beta cyclodextrin and citric acid show yield of K/S value, dry crease recovery angle and better retention of tensile strength than the two stage conventional method. FTIR spectra confirm that crosslinking successfully formed among the carboxyl group of citric acids and hydroxyl groups of cellulose and beta cyclodextrin forming ester crosslinks. Jasmine oil was also applied on cotton with beta cyclodextrin by micro encapsulation technique and without beta cyclodextrin by normal pad-dry-cure method. Jasmine oil applied with beta cyclodextrin by microencapsulation show higher level of retention of fragrance intensity for simultaneous in combined dyeing and finishing technique than two stage conventional methods. Human sensory evaluation indicates that fragrance intensity became gradually weaker with respect to time and higher nos. of washing cycle. Fragrance intensity after different duration of normal stoppage and also after nos. of wash cycles was tested by gas chromatography and, the fragrance intensity of Jasmine was found to be 15.88% after five repeat washing and the fragrance intensity was retained 39.5% in the cotton fabric up to 100 days of normal storing without washing. This single bath simultaneous reactive dyeing and aroma finishing also offers advantages of reduction of process cost, saving in energy, reduction in treatment time as well as better color yield and therefore is of commercial importance too.&picture=http://www.aascit.org/aascit/decorators/img/journal/891.jpg)
| [1] | A. K. Samanta, Department of Jute and Fibre Technology, Institute of Jute Technology, University of Calcutta 35 Ballygunge Circular Road, Kolkata, India. |
| [2] | Anowar Hossain, Department of Jute and Fibre Technology, Institute of Jute Technology, University of Calcutta 35 Ballygunge Circular Road, Kolkata, India. |
| [3] | A. Bagchi, Department of Jute and Fibre Technology, Institute of Jute Technology, University of Calcutta 35 Ballygunge Circular Road, Kolkata, India. |
| [4] | Kashmita Bhattacharya, Department of Jute and Fibre Technology, Institute of Jute Technology, University of Calcutta 35 Ballygunge Circular Road, Kolkata, India. |
A newer method of simultaneous dyeing and finishing has been developed using pad-dry-cure method by using limited aqueous solution of reactive dye, citric acid and suitable fragrance chemical microencapsulated in beta-cyclodextrin solubilized in PEG 200 and water (1:3) along with Citric acid and Sodium hypophosphite as catalyst applied on cotton fabric by pad-dry-cure method. Spectrophotometer analysis of combined dyed and finished cotton fabric show a deeper color yield and good aroma finishing using monochlorotriazine reactive dye along with jasmine oil microencapsulated in beta cyclodextr in in presence of citric acid and sodium hypophosphite applied on cotton fabric. For comparison purpose, beta cyclodextrin encapsulated aroma finish was also applied after dyeing cotton fabric with the same monochlorotriazine on cotton fabric in conventional two stage process. Simultaneous reactive dyeing and aroma finishing with beta cyclodextrin and citric acid show yield of K/S value, dry crease recovery angle and better retention of tensile strength than the two stage conventional method. FTIR spectra confirm that crosslinking successfully formed among the carboxyl group of citric acids and hydroxyl groups of cellulose and beta cyclodextrin forming ester crosslinks. Jasmine oil was also applied on cotton with beta cyclodextrin by micro encapsulation technique and without beta cyclodextrin by normal pad-dry-cure method. Jasmine oil applied with beta cyclodextrin by microencapsulation show higher level of retention of fragrance intensity for simultaneous in combined dyeing and finishing technique than two stage conventional methods. Human sensory evaluation indicates that fragrance intensity became gradually weaker with respect to time and higher nos. of washing cycle. Fragrance intensity after different duration of normal stoppage and also after nos. of wash cycles was tested by gas chromatography and, the fragrance intensity of Jasmine was found to be 15.88% after five repeat washing and the fragrance intensity was retained 39.5% in the cotton fabric up to 100 days of normal storing without washing. This single bath simultaneous reactive dyeing and aroma finishing also offers advantages of reduction of process cost, saving in energy, reduction in treatment time as well as better color yield and therefore is of commercial importance too.
Keywords
Simultaneous Dyeing and Finishing, Reactive Dyeing, Aroma Finishing, Beta Cyclodextrin & Microencapsulation
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